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KMID : 1059519850290040437
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Journal of the Korean Chemical Society
1985 Volume.29 No. 4 p.437 ~ p.440
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Amination of Organic Azides using Tetracarbonylhydridoferrate(O) as a Reducing Agent(I)
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Shim Sang-Chul
Choi Kui-Nam
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Abstract
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Organic azides were reduced to organic amines in the presence of tetracarbonylhydridoferrate(O) as a highly selective reducing agent at room temperature under carbon monoxide atmosphere. Particularly, benzoylazide gave ethylphenylcarbamate at room temperature but gave benzamide quantitatively at -40℃ in the presence of tetracarbonylhydridoferrate under carbon monoxide atmosphere.
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